反应条件
1: 90 percent / LAH / 1.) ether, 1h, reflux, 2.) rt
2: Br2, / CCl4
3: 74 percent / NaNH2, NH3 / tetrahydrofuran / 2 h
4: 97 percent / H2 / ethylendiamine poisoned P-2 Ni / ethanol
5: 85 percent / pyridine / 1 h / Ambient temperature
View Scheme
参考文献
Chattopadhyay, S.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 3 p. 236 - 237