1-甲氧基-4-对甲苯氧基苯合成路线 （共 26 条）
反应条件
2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=135°C; 36 h; Inert atmosphereSealed tube;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S)
Patent: US2011/306782 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=135°C; 36 h; Inert atmosphere;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S)
Patent: US2011/306782 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
copper(l) iodide; 5,6,9,10-tetrahydro-4H,8H-pyrido[3,2,1-ij][1,6]naphthyridine; caesium carbonate in toluene T=110°C; post-Ullmann reaction; 40 h;
参考文献
Wong, Ken-Tsung; Ku, Sung-Yu; Yen, Feng-Wen
Tetrahedron Letters, 2007 , vol. 48, # 29 p. 5051 - 5054
反应条件
potassium phosphate; 2-((o-toluidino)methyl)phenol; copper(l) chloride in acetonitrile T=81°C; Ullmann Condensation; 24 h; Schlenk techniqueInert atmosphere; Catalytic behavior;
参考文献
Qian, Cunwei; Qin, Liang; Zong, Qianshou; Wu, Lin; Fang, Dong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 12 p. 3915 - 3918
反应条件
potassium phosphate; 2-((o-toluidino)methyl)phenol; copper(l) chloride in acetonitrile T=81°C; Ullmann Condensation; 24 h; Schlenk techniqueInert atmosphere; Catalytic behavior;
参考文献
Qian, Cunwei; Qin, Liang; Zong, Qianshou; Wu, Lin; Fang, Dong
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 12 p. 3915 - 3918
反应条件
sodium methylate in pyridine
参考文献
American Home Products Corporation
Patent: US5169844 A1, 1992 ;
US 5169844 A
反应条件
bis(μ-iodo)bis[(-)-sparteine]-dicopper(I); potassium carbonate in dimethyl sulfoxide T=80°C; 12 h;
参考文献
Satyanarayana, Ponnam; Maheswaran, Hariharasarma; Kantam, Mannepalli Lakshmi; Bhargava, Suresh
Bulletin of the Chemical Society of Japan, 2011 , vol. 84, # 7 p. 788 - 790
反应条件
copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide T=100°C; 8 h;
参考文献
Cui, Sun-Liang; Jiang, Zhi-Yong; Wang, Yan-Guang
Synlett, 2004 , # 10 p. 1829 - 1831
反应条件
potassium carbonate in acetonitrile T=50°C; 24 h;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
反应条件
potassium carbonate in acetonitrile T=50°C; 24 h; regioselective reaction;
参考文献
Kakinuma, Yohji; Moriyama, Katsuhiko; Togo, Hideo
Synthesis (Germany), 2013 , vol. 45, # 2 art. no. SS-2012-F0786-OP, p. 183 - 188
