2,5-二甲基-2-己烯合成路线 （共 31 条）
反应条件
1: T=20°C; P=3863.02 Torr; Molecular sieve; 2: With nitrobenzene; tetrachloro-.pi.-diisobutylene dipalladium(II) 48 h; Inert atmosphere;
参考文献
WO2011/44243 A1, ;
Page/Page column 42 ;
反应条件
hydrogen; poly-1,2,3-triazolyl ferrocenyl dendrimer-Pd nanoparticle in methanol; chloroform T=25°C; P=760.051 Torr;
参考文献
Chemistry - A European Journal, , vol. 14, # 1 p. 50 - 64
反应条件
1: tert-butyl hyponitrite, triethylamine / dimethyl ether / 1 h / -78 °C 2: hexane / -10 °C / other solvents, temperatures; Ea, log A, ΔH<*>, ΔS<*>, ET, ΔG<*> View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 3 p. 766 - 773
反应条件
1: 34 percent / lithium aluminium hydride / diethyl ether; dibutyl ether / 4 h / Heating 2: tert-butyl hyponitrite, triethylamine / dimethyl ether / 1 h / -78 °C 3: hexane / -10 °C / other solvents, temperatures; Ea, log A, ΔH<*>, ΔS<*>, ET, ΔG<*> View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 3 p. 766 - 773
反应条件
1: 90 percent / sodium nitrite / H2O / 72 h / 85 °C 2: 34 percent / lithium aluminium hydride / diethyl ether; dibutyl ether / 4 h / Heating 3: tert-butyl hyponitrite, triethylamine / dimethyl ether / 1 h / -78 °C 4: hexane / -10 °C / other solvents, temperatures; Ea, log A, ΔH<*>, ΔS<*>, ET, ΔG<*> View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 3 p. 766 - 773
反应条件
in monofluoro-trichloromethane T=-78°C; Irradiation1.) 140 deg C, benzene; 2.) -78 deg C, irradiation, CH2Cl2, thioxanthone; Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 104, # 24 p. 6660 - 6668
反应条件
in monofluoro-trichloromethane T=-78°C; 12 h; Irradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 104, # 24 p. 6660 - 6668
反应条件
chromium corundum T=450°C; Inert atmosphere; Product distribution / selectivity;
参考文献
US2012/271082 A1, ;
Page/Page column 6-7 ;
反应条件
ethanol; palladium Hydrogenation;
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 422,423,428,430;engl.Ausg.S.409
反应条件
copper(II) sulfate T=185 - 205°C;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 197, p. 1435
Bulletin de la Societe Chimique de France, , vol. <5>9, p. 900
