3-苯基-1,2,4-三唑-5-硫醇水合物合成路线 （共 27 条）
反应条件
sodium hydroxide 0.05 h; microwave irradiation;
参考文献
Wang; Shi
Synthetic Communications, 2001 , vol. 31, # 18 p. 2841 - 2848
反应条件
tetraphosphorus decasulfide T=130 - 140°C; 6 h;
参考文献
Singh, Harjit; Sarin, Rakesh
Tetrahedron, 1986 , vol. 42, # 5 p. 1449 - 1460
反应条件
sodium hydroxide in ethanol 6 h; Heating;
参考文献
Heydenhauss, Dietrich; Jaenecke, Guenter; Feuerstein, Bernd
Zeitschrift fuer Chemie (Stuttgart, Germany), 1981 , vol. 21, # 1 p. 31 - 32
反应条件
ammonium thiocyanate 1.) 170 - 180 deg C, 1 h, 2.) 20 percent NaOH, reflux, 1 h; Multistep reaction;
参考文献
Pharmazie, , vol. 46, # 2 p. 109 - 112
反应条件
hydrogenchloride; acetic acid; zinc 1) reflux, 0.5 h 2) reflux, 1 h;
参考文献
Dash, B.; Dora, E. K.; Panda, C. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 834 - 835
反应条件
1: Hydrazine hydrate / ethanol / Heating 2: HCl(conc) / methanol / 4 h / Heating 3: aq. NaOH / 4 h / Heating View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 19, # 4 p. 260 - 262
反应条件
1: 75 percent / Pb(OAc)4 / CH2Cl2 / 1.5 h 2: 42 percent / 1) Zn, HOAc 2) conc.HCl / 1) reflux, 0.5 h 2) reflux, 1 h View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, # 1-12 p. 834 - 835
反应条件
1: pyridine / 24 h / 0 - 20 °C 2: sodium / ethanol / Reflux View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 1 p. 380 - 386
参考文献
Australian Journal of Chemistry, , vol. 61, # 5 p. 332 - 341
反应条件
Cadmium acetate in 1,4-dioxane; water T=180°C; P=12160 Torr; 3 h;
参考文献
Trzhtsinskaya, B. V.; Rudakova, E. V.; Afonin, A. V.; Voronov, V. K.; Pertsikov, B. Z.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 12 p. 2516 - 2518
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 12 p. 2745 - 2747
