1,2-dibromoethane; chlorotrimethylsilane in tetrahydrofuran charging of Schlenk flask with Zn (1.4 equiv.) under Ar, addn. of THF, addn. of 1,2-dibromoethane, boiling, addn. of SiClMe3, boiling, addn. of 1-iodobutane (1 equiv.), stirring overnight at room temp.;
参考文献
Fleckenstein, Julia E.; Koszinowski, Konrad
Organometallics, 2011 , vol. 30, # 18 p. 5018 - 5026
Yoshioka
Yakugaku Zasshi, 1955 , vol. 75, p. 606
Chem.Abstr., 1956 , p. 795
Full Text Show Details
Moroe
Yakugaku Zasshi, 1950 , vol. 70, p. 416,422
Yakugaku Zasshi, 1951 , vol. 71, p. 123
