甲基3-巯基-D-缬氨酸酯盐酸盐合成路线 (共 7 条)
反应条件
thionyl chloride 120 h; in a sealed vessel;
参考文献
Buchanan, Iain; Garner, C. David; Clegg, William
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 1333 - 1342
反应条件
1: conc. hydrochloric acid / H2O / 0.15 h / Heating 2: hydrogen chloride / r.t. 16 h; reflux, 2.5 h View Scheme
参考文献
Wolfe; Bowers; Hasan; Kazmaier
Canadian Journal of Chemistry, 1981 , vol. 59, # 2 p. 406 - 421
反应条件
hydrogenchloride r.t. 16 h; reflux, 2.5 h; Yield given;
参考文献
Wolfe; Bowers; Hasan; Kazmaier
Canadian Journal of Chemistry, 1981 , vol. 59, # 2 p. 406 - 421
反应条件
sodium acetate dextrorotatory substance;
参考文献
Sheehan; Bose
Journal of the American Chemical Society, 1952 , vol. 74, p. 4957
反应条件
2: aqueous KOH
View Scheme
参考文献
Cook; Heilbron
Chem. Penicillin, <Princeton 1949>, S. 921, 959
反应条件
triethylamine in dichloromethane
T=25°C; 48 h;
参考文献
Eggleton, Gordon L.; Bushman, Daniel R.; Whitlock, David W.; Pugh, Darrell K.; Chance, Katherine L.
Journal of Chemical & Engineering Data, 1984 , vol. 29, # 3 p. 351 - 354
反应条件
triethylamine in dichloromethane
T=25°C; 48 h;
参考文献
Eggleton, Gordon L.; Bushman, Daniel R.; Whitlock, David W.; Pugh, Darrell K.; Chance, Katherine L.
Journal of Chemical & Engineering Data, 1984 , vol. 29, # 3 p. 351 - 354