N-苯甲酰基-beta-丙氨酸合成路线 (共 24 条)
反应条件
1: NaOH / methanol 2: SOCl2 View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 98, p. 1014 - 1030
反应条件
n-butyllithium; naphthalenyllithium 1.) THF, ether, -78 deg C, 20 min 2.) THF, 5 h, -78 deg C; 3.) 20 deg C; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 29, # 23 p. 2859 - 2860
参考文献
Gazzetta Chimica Italiana, , vol. 98, p. 1014 - 1030
参考文献
Helvetica Chimica Acta, , vol. 9, p. 338
反应条件
T=110°C; 0.166667 h;
参考文献
Nandi, M. M.; Ray, Ruma
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 222 - 224
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1.) 0 deg C, 30 min, 2.) room temperature, overnight, 3.) reflux, 9 h;
参考文献
Sammes, Peter G.; Smith, Steven
Journal of the Chemical Society, Chemical Communications, 1983 , # 12 p. 682 - 684
反应条件
diphenylphosphoranyl azide; triethylamine; benzyl alcohol 1.) benzene, reflux, 30 min, 2.) reflux, overnight; Yield given. Multistep reaction;
参考文献
Olsen; Hennen; Wardle
Journal of Organic Chemistry, 1982 , vol. 47, # 24 p. 4605 - 4611
参考文献
Kametani; Kano
Yakugaku Zasshi, 1951 , vol. 71, p. 1007
Chem.Abstr., 1952 , p. 8121
反应条件
methanol; sodium methylate Electrolysis;
参考文献
Linstead et al.
Journal of the Chemical Society, 1951 , p. 2854,2856
反应条件
thionyl chloride Behandeln des erhaltenen Saeurechlorids mit Ammoniak in Chloroform;
参考文献
Kanewskaja
Chemische Berichte, 1936 , vol. 69, p. 266,270