5-苯基二硫杂环戊烯-3-硫酮合成路线 （共 57 条）
参考文献
Boettcher; Bauer
Justus Liebigs Annalen der Chemie, 1950 , vol. 568, p. 227,237
参考文献
Thuillier; Vialle
Bulletin de la Societe Chimique de France, 1959 , p. 1398,1400
参考文献
Lozac'h et al.
Bulletin de la Societe Chimique de France, 1953 , p. 1016,1017, 1019
反应条件
chloroform; mercury(II) diacetate; acetic acid
参考文献
Boberg, Friedrich; Puttins, Udo; Schmidt, Wolfgang; Torges, Karl-Franz
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 17, p. 135 - 140
参考文献
Woronkow; Broun; Karpenko
Zhurnal Obshchei Khimii, 1949 , vol. 19, p. 1927,1939
Chem.Abstr., 1950 , p. 1955
参考文献
Boettcher
Chemische Berichte, 1948 , vol. 81, p. 376
反应条件
1: 1.) thiophosgen / 1.) toluol, reflux, 2h; 2.) acetic acid, 80 deg C, 0.5 h
2: Br2 / CCl4 / 3 h / Heating
3: benzene; methanol / Ambient temperature; overnight
4: 0.5 h / 160 °C
5: 1.) KOH, 2.) 2 N H2SO4 / methanol; H2O / 3 h / Heating
View Scheme
参考文献
Boberg, Friedrich; Puttins, Udo; Schmidt, Wolfgang; Torges, Karl-Franz
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 17, p. 135 - 140
