暂无反应条件数据

in ethanol Condensation;

zirconium(IV) oxychloride octahydrate in ethanol 8 h; Inert atmosphereReflux;

ammonium hydroxide in ethanol; water addn. of hot soln. of Schiff base in EtOH to soln. of Ce salt in EtOH (ratio 1 : 1), addn. of H2O and EtOH (to 85percent EtOH), pH adjusting to 5.0 - 6.0 (NH4OH), refluxing (2 h), concn. (vac.), crystn. on cooling (over night); filtration, washing (EtOH), recrystn. (hot DMF/EtOH), washing (EtOH, Et2O), drying (vac.); elem. anal.;

ammonium hydroxide in ethanol; water addn. of soln. of Ce salt in EtOH to hot soln. of Schiff base in EtOH (ratio 1 : 2), addn. of H2O and EtOH (to 85percent EtOH), pH adjusting to 5.0 - 6.0 (NH4OH), refluxing (2 h), concn. (vac.), crystn. on cooling (over night); filtration, washing (EtOH), recrystn. (hot DMF/EtOH), washing (EtOH, Et2O), drying (vac.); elem. anal.;