4,4'-二氟二苯甲酮合成路线 (共 115 条)
参考文献
Rev. Inst. SalubridadChem.Abstr., , vol. 8, p. 63,66
Rev. Inst. SalubridadChem.Abstr., , p. 1920
反应条件
air; Mn(III) acetylacetonate T=23°C; 12 h; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 6 p. 1800 - 1809
反应条件
NSC26899; oxygen in acetonitrile T=20°C; 2.5 h;
参考文献
Tetrahedron Letters, , vol. 46, # 34 p. 5739 - 5742
反应条件
in tetrahydrofuran T=-80 - 20°C; Inert atmosphere;
参考文献
Bottalico, Daniela; Fiandanese, Vito; Marchese, Giuseppe; Punzi, Angela
Synthesis, 2009 , # 14 art. no. T04309SS, p. 2316 - 2318
反应条件
1: 0.33 h / Reflux 2: Ru(bpy)3Cl2; caesium carbonate / N,N-dimethyl acetamide / 48 h / 25 °C / Irradiation View Scheme
参考文献
Organic Letters, , vol. 13, # 9 p. 2168 - 2171
反应条件
1.1: magnesium / tetrahydrofuran / 2 h / 20 - 85 °C 1.2: 0 - 20 °C / |Inert atmosphere 2.1: pyridinium chlorochromate; triethylamine / dichloromethane / 20 °C View Scheme
参考文献
Organic Letters, , vol. 14, # 18 p. 4850 - 4853,4
反应条件
oxygen; manganese triacetate in acetic acid T=32°C; 12 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 30, # 1 p. 209 - 216
参考文献
Journal of the American Chemical Society, , vol. 91, p. 3037 - 3044
反应条件
tetramethyl-ammonium fluoride; dimethyl sulfoxide T=100°C; 1 h; Yield given;
参考文献
Adams, Dave J.; Clark, James H.; McFarland, Heather
Journal of Fluorine Chemistry, 1998 , vol. 92, # 2 p. 127 - 129
反应条件
in acetonitrile Ambient temperatureBu4NBF4, nickel rod anode, nickel foam catode, 1.5 A/dm2;
参考文献
Folest, Jean-Claude; Pereira-Martins, Edouard; Troupel, Michel; Perichon, Jacques
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7571 - 7574