3-氨基-邻苯二甲酸二甲酯合成路线 （共 15 条）
反应条件
cyclohexene; palladium on activated charcoal in ethanol 3 h; Heating;
参考文献
Vinod, Thottumkara K.; Thottumkara, Arun P.
Patent: US2004/30187 A1, 2004 ;
Location in patent: Page 2; Sheet 1 ;
反应条件
1: methanol; mononitrophthalic acid With thionyl chloride T=0°C; 9 h; RefluxInert atmosphere; 2: ethyl iodide With potassium carbonate in N,N-dimethyl-formamide T=80°C; 8 h; Inert atmosphere; 3: With 5 palladium on charcoal; hydrogen in methanol; water T=20°C; 5 h;
参考文献
WO2013/97226 A1, ;
Page/Page column 48; 49 ;
反应条件
trifluoroacetic acid in tetrachloromethane 2 h; Heating;
参考文献
Differding, Edmond; Vandevelde, Oscar; Roekens, Bertrand; Van, Tran Trieu; Ghosez, Leon
Tetrahedron Letters, 1987 , vol. 28, # 4 p. 397 - 400
反应条件
1: SOCl2 / Heating 2: Heating 3: 100 percent / H2 / Pd-C / methanol / 2844.31 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 43, # 4 p. 569 - 572
反应条件
1: Heating 2: 100 percent / H2 / Pd-C / methanol / 2844.31 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 43, # 4 p. 569 - 572
参考文献
Blair et al.
Journal of the Chemical Society, 1958 , p. 304
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Blair et al.
Journal of the Chemical Society, 1958 , p. 304
参考文献
Blair et al.
Journal of the Chemical Society, 1958 , p. 304
反应条件
1: aqueous HCl; NaNO2 / anschliessend Behandeln mit CuCN 2: aqueous NaOH View Scheme
参考文献
Gut
Collection of Czechoslovak Chemical Communications, 1956 , vol. 21, p. 1648
反应条件
1.1: NaNO2; HCl / 0 - 5 °C 1.2: 91 percent / KI 2.1: 93 percent / NaOH / tetrahydrofuran; H2O View Scheme
参考文献
Thottumkara, Arun P; Vinod, Thottumkara K
Tetrahedron Letters, 2002 , vol. 43, # 4 p. 569 - 572
