potassium tert-butylate; hydrogen; RuCl2[(S)-DMM-SDP](R,R)-DACH in isopropyl alcohol T=20°C; P=375030 Torr; 8 h; Title compound not separated from byproducts;
参考文献
Giacomini, Daria; Galletti, Paola; Quintavalla, Arianna; Gucciardo, Gabriele; Paradisi, Francesca
Chemical Communications, 2007 , # 39 p. 4038 - 4040
1: RhCl(PPh3)3 / benzene / 24 h / Ambient temperature 2: 30percent KOH / methanol; H2O / 0.17 h View Scheme
参考文献
Maslinska-Solich, Jolanta; Rudnicka, Irena; Jedlinski, Zbigniew J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3034 - 3040
Adkins; Krsek
Journal of the American Chemical Society, 1949 , vol. 71, p. 3053
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McKenzie; Luis; Mitchell
Chemische Berichte, 1932 , vol. 65, p. 798,803