1-甲氧基-1-三甲基硅氧基丙烯合成路线 （共 16 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78°C; 3.5 h;
参考文献
Kita, Yasuyuki; Segawa, Jun; Haruta, Jun-ichi; Yasuda, Hitoshi; Tamura, Yasumitsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1099 - 1104
反应条件
zinc(II) chloride in dichloromethane Ambient temperature;
参考文献
Reetz, Manfred T.; Schwellnus, Konrad; Huebner, Friedhelm; Massa, Werner; Schmidt, Roland E.
Chemische Berichte, 1983 , vol. 116, # 11 p. 3708 - 3724
反应条件
in acetonitrile 1 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 62, # 9 p. 2742 - 2751
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 1 h;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 2 h;
参考文献
Kita, Yasuyuki; Yasuda, Hitoshi; Haruta, Jun-ichi; Segawa, Jun; Tamura, Yasumitsu
Synthesis, 1982 , # 12 p. 1089 - 1091
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 1 h;
参考文献
Synthesis, , # 12 p. 1089 - 1091
反应条件
in benzene 4.5 h; PhotolysisInert atmosphere; regioselective reaction;
参考文献
Cho, Dae Won; Park, Hea Jung; Yoon, Ung Chan; Lee, Hyang-Yeol; Mariano, Patrick S.
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10304 - 10313
反应条件
in acetonitrile 1 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 62, # 9 p. 2742 - 2751
反应条件
trimethylsilyl trifluoromethanesulfonate in chloroform
T=0°C; Sakurai-Hosomi reaction; 1 h;
参考文献
Kobashi, Yohei; Minowa, Tomofumi; Mukaiyama, Teruaki
Chemistry Letters, 2005 , vol. 34, # 6 p. 756 - 757
反应条件
(R)-(S)-(4-MeO-3,5-Me2C6H2)2PC5H3CH(CH3)P(C6H11)2)Fe(C5H5); palladium diacetate; thallous acetate in toluene
T=70°C; 6 h; optical yield given as percent eeenantioselective reaction;
参考文献
Kobayashi, Kenya; Yamamoto, Yasunori; Miyaura, Norio
Organometallics, 2011 , vol. 30, # 22 p. 6323 - 6327
