4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Hicks, Jacqueline D.; Hyde, Alan M.; Cuezva, Alberto Martinez; Buchwald, Stephen L.
Journal of the American Chemical Society, 2009 , vol. 131, # 46 p. 16720 - 16734
Zahn; Zuber
Chemische Berichte, 1953 , vol. 86, p. 172,180
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Lichtenberger; Thermet
Bulletin de la Societe Chimique de France, 1951 , p. 318,323
1: 60 percent / H2S, aq. KOH / 3 h / 20 - 25 °C 2: 55 percent / tBuOK, Adogen-464 / various solvent(s) / 15 h / Ambient temperature 3: 2-(phenylsulfonyl)-3-(p-nitrophenyl)oxaziridine / CDCl3 View Scheme
参考文献
Davis, Franklin A.; Ray, Jayanta K.; Kasperowicz, Steve; Przeslawski, Robert M.; Durst, H. Dupont
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2594 - 2599