N1-[4-(三氟甲基0苯基]乙酰氨合成路线 （共 34 条）
反应条件
[bis(acetoxy)iodo]benzene; silver fluoride in dimethyl sulfoxide T=20°C; 20 h;
参考文献
Chemical Communications, , vol. 49, # 57 p. 6385 - 6387
反应条件
tert.-butylhydroperoxide; copper(II) bis(trifluoromethanesulfonate) in water; acetonitrile T=20°C; 2.5 h; other aromatic compounds; Mechanism;
参考文献
Tetrahedron Letters, , vol. 32, # 51 p. 7525 - 7528
反应条件
1.1: tert.-butylnitrite / water; ethanol / 1 h / 0 - 20 °C / |Inert atmosphere 2.1: copper(I) isothiocyanate; caesium carbonate / acetonitrile / 0.17 h / 20 °C / |Inert atmosphere 2.2: 16 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 31 p. 7972 - 7975
Angew. Chem., , vol. 125, # 31 p. 8130 - 8133
反应条件
T=150°C; microwave irradiation;
参考文献
Wang, Xiao-Jian; Yang, Qian; Liu, Fei; You, Qi-Dong
Synthetic Communications, 2008 , vol. 38, # 7 p. 1028 - 1035
反应条件
in acetonitrile 4.5 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 2 p. 447 - 452
反应条件
thionyl chloride in methanol 2.5 h; Reflux;
参考文献
Wang, Gong-Bao; Wang, Lin-Fa; Li, Chao-Zhang; Sun, Jing; Zhou, Guang-Ming; Yang, Da-Cheng
Research on Chemical Intermediates, 2012 , vol. 38, # 1 p. 77 - 89
反应条件
1: 8.7 g / fluoroxytrifluoromethane, AcOH / 8 h 2: 88 percent / HCl / ethanol / 1 h / Heating View Scheme
参考文献
Fifolt, Michael J.; Olczak, Raymond T.; Mundhenke, Rudolph F.
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4576 - 4582
反应条件
1: K2CO3, CuBr, Cu, KI / Heating 2: aq. HCl / ethanol 3: aq. Na2CO3 View Scheme
参考文献
Kozachuk,D.N. et al.
Zhurnal Organicheskoi Khimii, 1974 , vol. 10, # 6 p. 1230 - 1236,1239 - 1243
反应条件
copper(l) iodide; copper; potassium carbonate in nitrobenzene
17 h; Heating;
参考文献
Dapperheld, Steffen; Steckhan, Eberhard; Grosse Brinkhaus, Karl-Heinz; Esch, Thomas
Chemische Berichte, 1991 , vol. 124, # 11 p. 2557 - 2568
反应条件
und anschliessende Hydrolyse mit aethanol.KOH;
参考文献
Roe et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 28,29
