3-二甲基氨基-1-苯丙烷-1-酮合成路线 （共 69 条）
反应条件
1: methanol. sodium methylate 2: aqueous hydrochloric acid; amalgamated zinc View Scheme
参考文献
Reichert; Posemann
Archiv der Pharmazie (Weinheim, Germany), 1937 , vol. 275, p. 67,78
参考文献
Mannich; Heilner
Chemische Berichte, 1922 , vol. 55, p. 362
反应条件
1.1: 93 percent / trans-RuCl2[(S)-xylbinap][(S)-daipen]; t-BuOK; H2 / propan-2-ol; 2-methyl-propan-2-ol / 5 h / 25 °C / 6080.41 Torr 2.1: NaH / dimethylformamide / 0.5 h / 90 °C 2.2: 100 percent / dimethylformamide / 1 h / 100 °C 3.1: 96 percent / α-chloroethyl chloroformate / 1,2-dichloro-ethane / 1.33 h / 0 - 50 °C View Scheme
参考文献
Ohkuma, Takeshi; Ishii, Dai; Takeno, Hiroshi; Noyori, Ryoji
Journal of the American Chemical Society, 2000 , vol. 122, # 27 p. 6510 - 6511
参考文献
Nomura et al.
Kogyo Kagaku Zasshi, 1956 , vol. 59, p. 384
Chem.Abstr., 1957 , p. 11354
Full Text Show Details
Oda et al.
Bl.Inst.chem.Res.Kyoto Univ., 1956 , vol. 34, p. 224,226
反应条件
dichloro bis(acetonitrile) palladium(II) in acetonitrile
Heating;
参考文献
Murahashi, Shun-Ichi; Tsumiyama, Tatsuo; Mitsue, Yo
Chemistry Letters, 1984 , p. 1419 - 1422
参考文献
Jacob; Madinaveitia
Journal of the Chemical Society, 1937 , p. 1929
Full Text Show Details
Duffin; Kendall
Journal of the Chemical Society, 1954 , p. 408,411
Journal of the Chemical Society, 1955 , p. 3470,3473
参考文献
Surya Prakash Rao; Jeyalakshmi; Senthilkumar
Tetrahedron, 2002 , vol. 58, # 11 p. 2189 - 2199
反应条件
T=20°C; 24 h; Ionic liquid;
参考文献
Rashinkar, Gajanan; Pore, Santoshkumar; Salunkhe, Rajeshree
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 7 p. 1750 - 1758
参考文献
Surya Prakash Rao; Jeyalakshmi; Senthilkumar
Tetrahedron, 2002 , vol. 58, # 11 p. 2189 - 2199
参考文献
Austin,E.M. et al.
Tetrahedron, 1969 , vol. 25, p. 5509 - 5516
