Ye, Mengchun; Gao, Guo-Lin; Edmunds, Andrew J. F.; Worthington; Morris, James A.; Yu, Jin-Quan
Journal of the American Chemical Society, 2011 , vol. 133, # 47 p. 19090 - 19093
1: With 2,2,6,6-tetramethyl-piperidine; n-butyllithium; tri-isopropoxy-borane in tetrahydrofuran; hexane
T=-78 - -40°C; 4 h;
2: With hydrogenchloride in tetrahydrofuran; hexane; water
参考文献
ELI LILLY AND COMPANY
Patent: WO2005/94822 A1, 2005 ;
Location in patent: Page/Page column 32 ;
WO 2005/094822 A1