2-[(苯基氨基)甲基]苯酚合成路线 (共 35 条)
反应条件
Bu2SnClH-HMPA in tetrahydrofuran T=0°C; 1 h;
参考文献
Shibata, Ikuya; Suwa, Toshihiro; Sugiyama, Erika; Baba, Akio
Synlett, 1998 , # 10 p. 1081 - 1082
反应条件
sodium tetrahydroborate in methanol T=0°C; 0.666667 h;
参考文献
Tang, Zilong; Chen, Weiwen; Zhu, Zhonghua; Liu, Hanwen
Journal of Heterocyclic Chemistry, 2011 , vol. 48, # 2 p. 255 - 260
反应条件
hydrogen in ethanol T=20°C; 6 h; Milling;
参考文献
Zhou, Jinghui; Dong, Zhengping; Wang, Peng; Shi, Zhiqiang; Zhou, Xingchun; Li, Rong
Journal of Molecular Catalysis A: Chemical, 2014 , vol. 382, p. 15 - 22
反应条件
1: in toluene T=100°C; Diels-Alder reaction; 8 h; 2: With hydrogenchloride in tetrahydrofuran 2 h; Further stages.;
参考文献
Sugimoto, Hiromichi; Nakamura, Satoshi; Ohwada, Tomohiko
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 4-5 p. 669 - 679
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; di-n-butylchlorotin hydride in tetrahydrofuran T=0°C; Reduction; Amination; 1 h;
参考文献
Suwa, Toshihiro; Sugiyama, Erika; Shibata, Ikuya; Baba, Akio
Synthesis, 2000 , # 6 p. 789 - 800
反应条件
tetrahydrofuran; titanium(III) chloride; potassium chloride; lithium T=25°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 42, # 51 p. 9093 - 9095
反应条件
in acetonitrile T=80°C; 12 h;
参考文献
Modica; Zanaletti; Freccero; Mella
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 41 - 52
反应条件
9-borabicyclo[3.3.1]nonane dimer in benzene T=50°C;
参考文献
Kliegel, Wolfgang; Nanninga, Dierk
Journal of Organometallic Chemistry, 1983 , vol. 243, # 4 p. 373 - 386
反应条件
1: ethanol / 3 h / Reflux 2: sodium tetrahydroborate / methanol / 0.67 h / 0 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 48, # 2 p. 255 - 260
反应条件
1: ethanol / 3 h / Reflux 2: sodium tetrahydroborate / methanol / 0.67 h / 0 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 48, # 2 p. 255 - 260