2-碘-1,1,1-三氟乙烷合成路线 （共 59 条）
反应条件
potassium fluoride in dimethyl sulfoxide T=120 - 130°C; 4 h;
参考文献
Kamal, Ahmed; Pratap; Ramana, K.Venkata; Ramana; Babu, A.Hari
Tetrahedron Letters, 2002 , vol. 43, # 41 p. 7353 - 7355
反应条件
potassium carbonate in water; N,N-dimethyl-formamide
参考文献
Tularik Inc.
Patent: US2002/169159 A1, 2002 ;
US 20020169159 A1
反应条件
sodium hydride in various solvent(s) T=120°C; 18 h;
参考文献
Hammond, Gerald B.; Plevey, Raymond G.; Sampson, Paul; Tatlow, John Colin
Journal of Fluorine Chemistry, 1988 , vol. 40, p. 81 - 98
反应条件
diethyl ether; magnesium
参考文献
Journal of the American Chemical Society, , vol. 65, p. 2038
参考文献
Journal of the American Chemical Society, , vol. 65, p. 2038
反应条件
sodium hydride in pyridine T=20°C; 2 h; Product distribution / selectivity;
参考文献
US2008/306308 A1, ;
Page/Page column 7-8 ;
反应条件
in hexane T=293°C; Rate constant;
参考文献
Jones, Michelle B.; Maloney, Vincent M.; Platz, Matthew S.
Journal of the American Chemical Society, 1992 , vol. 114, # 6 p. 2163 - 2169
反应条件
potassium carbonate in dimethyl sulfoxide T=120°C; 6 h;
参考文献
SANDOZ AG
Patent: US2012/165548 A1, 2012 ;
Location in patent: Page/Page column 11 ;
反应条件
potassium fluoride in dimethyl sulfoxide T=120 - 130°C; 4 h;
参考文献
Kamal, Ahmed; Pratap; Ramana, K.Venkata; Ramana; Babu, A.Hari
Tetrahedron Letters, 2002 , vol. 43, # 41 p. 7353 - 7355
反应条件
potassium carbonate in water; N,N-dimethyl-formamide
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: US5387603 A1, 1995 ;
