in tetrahydrofuran a soln. of CH2CHMgCl allowed to stand for 24 h, the upper layer decantedto the reaction flask, a soln. of GeCl4 added at a temp. not exceeding 30°C, kept at 20-30°C for 6 h; treated with H2O, the aq. layer sepd., the org. layer washed (H2O), distd. fractionally;
参考文献
Zhun'; Sbitneva; Kisin; Chernyshev
Russian Journal of General Chemistry, 2004 , vol. 74, # 7 p. 1130 - 1131
Kato, Tetsuya; Kondo, Hisao; Nishino, Masaki; Tanaka, Minoru; Hata, Go; Miyake, Akihisa
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 10 p. 2958 - 2961
