1,1,1,2,3,4,4,4-八氟-2,3-二(三氟甲基)丁烷合成路线 (共 22 条)
参考文献
Rosenberg, R. M.; Muetterties, E. K.
Inorganic Chemistry, 1962 , vol. 1, p. 756 - 762
参考文献
Miller
Patent: US2716141 , 1950 ;
反应条件
in 1,2,2-trifluoro-trichloroethane 48 h; Ambient temperature;
参考文献
Chengxue, Zhao; Renmo, Zhou; Heqi, Pan; Xiangshan, Jin; Yangling, Qu; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2009 - 2013
反应条件
1: coppered zinc; dioxane 2: fluorine View Scheme
参考文献
Miller
Patent: US2716141 , 1950 ;
反应条件
byproducts: SiF4; at 420 Torr and 200°C (1 h);
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.11.1, page 149 - 158
反应条件
cobalt(III) fluoride T=360°C; 3 h; Product distribution;
参考文献
Burdon, James; Creasey, Jeremy C.; Proctor, Lee D.; Plevey, Raymond G.; Yeoman, J.R. Neil
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 445 - 447
反应条件
Irradiationeffect of the reaction temp. and time; Equilibrium constantProduct distribution;
参考文献
Voehringer, Cecilia M. de; Staricco, Eduardo H.
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1984 , vol. 80, p. 2631 - 2638
反应条件
cobalt(III) fluoride T=360°C; 3 h; Product distribution;
参考文献
Burdon, James; Creasey, Jeremy C.; Proctor, Lee D.; Plevey, Raymond G.; Yeoman, J.R. Neil
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 4 p. 445 - 447
反应条件
T=249.85°C; Decomposition; 4 h;
参考文献
Scherer Jr.; Batt; Stewart
International Journal of Chemical Kinetics, 1994 , vol. 26, # 1 p. 73 - 83
反应条件
byproducts: SO2; with excess of HF, in bomb, one week, room temp.;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.5, page 187 - 208