2,4,6-三羟基二苯甲酮合成路线 (共 23 条)
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride Erhitzen des Reaktionsprodukts mit Wasser;
参考文献
Hoesch
Chemische Berichte, 1915 , vol. 48, p. 1125
参考文献
Harris,T.M.; Wachter,M.P.
Tetrahedron, 1970 , vol. 26, p. 5255 - 5263
反应条件
1: AlCl3; diethyl ether 2: ethanolic HCl View Scheme
参考文献
Phadke; Shah
Journal of the Indian Chemical Society, 1950 , vol. 27, p. 349,353
反应条件
acridone synthase from Citrus Microcarpa pH=6.5 - 8.5; Enzymatic reaction;
参考文献
Mori, Takahiro; Shimokawa, Yoshihiko; Matsui, Takashi; Kinjo, Keishi; Kato, Ryohei; Noguchi, Hiroshi; Sugio, Shigetoshi; Morita, Hiroyuki; Abe, Ikuro
Journal of Biological Chemistry, 2013 , vol. 288, # 40 p. 28845 - 28858
反应条件
acetic anhydride 24 h; Heating;
参考文献
Ulubelen, Ayhan; Kerr, Robert R.; Mabry, Tom J.
Phytochemistry (Elsevier), 1982 , vol. 21, # 5 p. 1145 - 1148
参考文献
Hoesch
Chemische Berichte, 1915 , vol. 48, p. 1125
反应条件
phosphoric acid in xylene
T=30 - 35°C; 12 h;
参考文献
Ahluwalia, V. K.; Khanna, Manjula; Singh, Rishi P.
Synthesis, 1983 , # 5 p. 404 - 406
反应条件
N-ethyl-N,N-diisopropylamine in chloroform
T=20°C; 7 h;
参考文献
Brajeul, Solenn; Delpech, Bernard; Marazano, Christian
Tetrahedron Letters, 2007 , vol. 48, # 32 p. 5597 - 5600
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
T=20°C; 5.5 h; Further byproducts given;
参考文献
Cann, Martin R.; Davis, Anne-Marie; Shannon, Patrick V. R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 7 p. 1413 - 1421
参考文献
Spaeth; Fuchs
Monatshefte fuer Chemie, 1921 , vol. 42, p. 272