反应条件
in diethyl ether
reaction at -45°C, 0.75 hours (addition of CH3Li and ester drop by drop to n-C3F7I), stirring at -50 - -35°C, 36 hours and warming to 20°C, 24 hours, heating under reflux, 2 hours;;
参考文献
McBee et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 6387
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Gmelin Handbook: F: PerFHalOrg.4, 1.3.3.8, page 33 - 59
