1,5-二氯六甲基三硅氧烷合成路线 (共 36 条)
参考文献
Lebedev,E.P.; Valimukhametova,R.G.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, p. 233,217 - 218
参考文献
National Starch and Chemical Corporation
Patent: US4581461 A1, 1986 ;
参考文献
Volkova,L.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1963 , p. 1829 - 1831
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1963 , p. 1986 - 1989
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Andrianow; Dabagowa
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 1767,1768,1770;engl.Ausg.S.1693,1694,1696
反应条件
in acetic anhydride
T=30°C; Rate constant;
参考文献
Ruehlmann, K.
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 27, p. 139 - 152
参考文献
Lebedev,E.P.; Valimukhametova,R.G.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, p. 233,217 - 218
反应条件
pyridine; bis(trimethylsilyl)-sulfide; 1,3-dichloro-1,1,3,3-tetramethyldisiloxane
T=180 - 220°C; Yield given. Title compound not separated from byproducts;
参考文献
Mizhiritskii, M. D.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 7 p. 1537 - 1543,1367 - 1372