N-(吡啶-2-基甲基)苯甲酰胺合成路线 （共 8 条）
反应条件
1: in dichloromethane T=0°C; 0.5 h; 2: With triethylamine in dichloromethane T=20°C; 12.25 h;
参考文献
Srinivas, Keesara; Saiprathima, Parvathaneni; Balaswamy, Kodicherla; Ra, Mandapati Mohan
Journal of Organometallic Chemistry, 2013 , vol. 741-742, # 1 p. 162 - 167
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide T=70°C; P=30003 Torr; 48 h; AutoclaveInert atmosphere; TimeTemperaturePressure; chemoselective reaction;
参考文献
Gergely, Mate; Farkas, Roland; Takacs, Attila; Petz, Andrea; Kollar, Laszlo
Tetrahedron, 2014 , vol. 70, # 2 p. 218 - 224
反应条件
bis(trimethylaluminum)-1,4-diazabicyclo[2.2.2]octane in tetrahydrofuran T=130°C; 0.133333 h; Inert atmosphereMicrowave irradiation;
参考文献
Dubois, Nathalie; Glynn, Daniel; McInally, Thomas; Rhodes, Barrie; Woodward, Simon; Irvine, Derek J.; Dodds, Chris
Tetrahedron, 2013 , vol. 69, # 46 p. 9890 - 9897
反应条件
palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in CPME; water T=85°C; Suzuki-Miyaura cross-coupling; 24 h; Inert atmosphere;
参考文献
Molander, Gary A.; Hiebel, Marie-Aude
Organic Letters, 2010 , vol. 12, # 21 p. 4876 - 4879
反应条件
in toluene T=0°C; Inert atmosphere;
参考文献
Koch, Christian; Kahnes, Marcel; Schulz, Martin; Goerls, Helmar; Westerhausen, Matthias
European Journal of Inorganic Chemistry, 2008 , # 7 p. 1067 - 1077
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=0 - 20°C; Inert atmosphere;
参考文献
Hao, Xin-Qi; Chen, Li-Juan; Ren, Baozeng; Li, Liu-Yan; Yang, Xin-Yan; Gong, Jun-Fang; Niu, Jun-Long; Song, Mao-Ping
Organic Letters, 2014 , vol. 16, # 4 p. 1104 - 1107
反应条件
potassium carbonate T=160°C; 12 h;
参考文献
Cui, Xinjiang; Zhang, Yan; Shi, Feng; Deng, Youquan
Chemistry - A European Journal, 2011 , vol. 17, # 3 p. 1021 - 1028
反应条件
2-methoxy-pyridine; trifluoromethylsulfonic anhydride in dichloromethane T=35°C; 16 h; Inert atmosphere; ConcentrationReagent/catalystTemperatureTime;
参考文献
Pelletier, Guillaume; Charette, Andre B.
Organic Letters, 2013 , vol. 15, # 9 p. 2290 - 2293
