反式,反式-1,3-丁二烯-1,4-二羧酸合成路线 （共 65 条）
反应条件
Erwaermen des Reaktionsprodukts mit methanol. Kalilauge.;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 571, p. 44,55
反应条件
1: SOCl2 / 72 h / Heating 2: Et3N / toluene / 1 h / 0 °C 3: 97 percent / DIBAL-H / hexane; CH2Cl2 / 1 h / -78 °C View Scheme
参考文献
Barrett, Anthony G. M.; Doubleday, Wendel W.; Tustin, Gary J.
Tetrahedron, 1996 , vol. 52, # 48 p. 15325 - 15338
反应条件
1: SOCl2 / Erwaermen des Reaktionsprodukts mit Benzol und AlCl3 auf 50-60grad 2: benzene; platinum View Scheme
参考文献
Bailey; Ross
Journal of the American Chemical Society, 1949 , vol. 71, p. 2370
反应条件
potassium permanganate; osmium(VIII) oxide
参考文献
Behrend; Heyer
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 298,306
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Behrend
Chemische Berichte, 1916 , vol. 49, p. 1001
反应条件
sodium chlorate; osmium(VIII) oxide; acetic acid
参考文献
Behrend; Heyer
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 298,306
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Behrend
Chemische Berichte, 1916 , vol. 49, p. 1001
参考文献
Behrend; Heyer
Justus Liebigs Annalen der Chemie, 1919 , vol. 418, p. 298,306
Full Text Show Details
Behrend
Chemische Berichte, 1916 , vol. 49, p. 1001
参考文献
Moffett,L.R.; Hill,W.E.
Journal of Organic Chemistry, 1962 , vol. 27, p. 1454 - 1455
参考文献
Demole,E.; Stoll,M.
Helvetica Chimica Acta, 1962 , vol. 45, p. 692 - 703
反应条件
1: sulfuric acid / 16 h / Reflux 2: m-xylene / 48 h / 151 - 168 °C / 13446.2 Torr 3: hydrogen / palladium on activated charcoal / dichloromethane / 20 °C View Scheme
参考文献
AMYRIS, INC.; SCHWEITZER, Dirk, Ph.D.
Patent: WO2012/82725 A1, 2012 ;
反应条件
thionyl chloride; N,N-dimethyl-formamide in dichloromethane 10 h; Inert atmosphereReflux;
参考文献
Das, Swagatika; Das, Umashankar; Sakagami, Hiroshi; Umemura, Naoki; Iwamoto, Shoko; Matsuta, Tomohiko; Kawase, Masami; Molnar, Joseph; Serly, Julianna; Gorecki, Dennis K.J.; Dimmock, Jonathan R.
European Journal of Medicinal Chemistry, 2012 , vol. 51, p. 193 - 199
