2,3-二甲氧基-1,3-丁二烯合成路线 (共 31 条)
反应条件
sulfuric acid in methanol 12 h; Heating;
参考文献
Pozzo, Jean-Luc; Clavier, Gilles M.; Colomes, Michel; Bouas-Laurent, Henri
Tetrahedron, 1997 , vol. 53, # 18 p. 6377 - 6390
反应条件
sulfuric acid 10 h; Heating / reflux;
参考文献
COMMONWEALTH SCIENTIFIC AND INDUSTRIAL RESEARCH ORGANISATION
Patent: WO2008/31157 A1, 2008 ;
Location in patent: Page/Page column 60 ;
反应条件
sodium hydroxide; diethylene glycol monoethyl ether T=200°C;
参考文献
Journal of the American Chemical Society, , vol. 63, p. 135
反应条件
sodium hydroxide T=160°C;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 29, p. 197 - 205
参考文献
Journal of the American Chemical Society, , vol. 63, p. 135
反应条件
1: 19 percent / ozone / pentane / -30 °C 2: 56 percent / PPh3 / CDCl3 / 24 h View Scheme
参考文献
Griesbaum, Karl; Kim, Woo-Sun
Journal of Organic Chemistry, 1992 , vol. 57, # 21 p. 5574 - 5577
反应条件
SCl2; sodium acetate in hexane T=5 - 20°C;
参考文献
Von Kieseritzky, Fredrik; Allared, Fredrik; Dahlstedt, Emma; Hellberg, Jonas
Tetrahedron Letters, 2004 , vol. 45, # 31 p. 6049 - 6050
反应条件
beim Behandeln mit verduennten Mineralsaeuren;
参考文献
Johnson; Jobling; Bodamer
Journal of the American Chemical Society, 1941 , vol. 63, p. 134
参考文献
Johnson; Jobling; Bodamer
Journal of the American Chemical Society, 1941 , vol. 63, p. 135
反应条件
ozone in pentane T=-30°C;
参考文献
Journal of Organic Chemistry, , vol. 57, # 21 p. 5574 - 5577