N-(2-氰基乙基)-邻苯二甲酰亚胺合成路线 （共 15 条）
反应条件
hydrazine in ethanol; water 0.25 h; Inert atmosphereReflux;
参考文献
Dawadi, Prativa B. S.; Lugtenburg, Johan
European Journal of Organic Chemistry, 2008 , # 13 p. 2288 - 2292
参考文献
Galat
Journal of the American Chemical Society, 1945 , vol. 67, p. 1414
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Chodroff; Klapp; Beckmann
Journal of the American Chemical Society, 1947 , vol. 69, p. 258
反应条件
hydrogenchloride; hydrogen; platinum(IV) oxide in ethanol
P=760 Torr;
参考文献
Prabhakaran; Woo; Yorgey; Gould
Journal of the American Chemical Society, 1988 , vol. 110, # 17 p. 5785 - 5791
反应条件
1: H2, conc. HCl / PtO2 / ethanol / 760 Torr
2: Et3N / CH2Cl2 / 24 h / Ambient temperature
3: 87 percent / Ac2O, sodium nitrite / acetic acid / 10 h / 0 °C
4: 0.78 g / Na2CO3 / CCl4 / 24 h / Heating
5: NaI / acetone / 20 h / Heating
View Scheme
参考文献
Martinkus; Tann; Gould
Tetrahedron, 1983 , vol. 39, # 21 p. 3493 - 3505
反应条件
hydrogenchloride; dithiophosphoric acid O,O-diethyl ester in ethyl acetate
T=20°C; 6 h;
参考文献
Imanishi, Naoki; Iwaoka, Kiyoshi; Koshio, Hiroyuki; Nagashima, Shin-Ya; Kazuta, Ken-Ichi; Ohta, Mitsuaki; Sakamoto, Shuichi; Ito, Hiroyuki; Akuzawa, Shinobu; Kiso, Tetsuo; Tsukamoto, Shin-Ichi; Mase, Toshiyasu
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 7 p. 1493 - 1502
