N,N-二乙基-2,2,2-三氟乙酰胺合成路线 (共 28 条)
反应条件
in diethyl ether T=-6 - 20°C; Inert atmosphere;
参考文献
Smith, David P.; Anderson, Jon; Plante, Jeffrey; Ashcroft, Alison E.; Radford, Sheena E.; Wilson, Andrew J.; Parker, Martin J.
Chemical Communications, 2008 , # 44 p. 5728 - 5730
参考文献
Ovchinnikova, N. S.; Veraksich, O. V.; Pospelov, M. V.; Zhuravlev, L. T.; Glazunov, M. P.; Fokin, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 4 p. 752 - 756
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 4 p. 827 - 832
反应条件
in benzene ice cooling;
参考文献
Horner, Leopold; Jordan, Manfred
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 235 - 242
参考文献
Journal of the American Chemical Society, , vol. 77, p. 6662
反应条件
0.333333 h; Ambient temperature;
参考文献
Horner, Leopold; Jordan, Manfred
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 235 - 242
反应条件
in diethyl ether T=20°C; Substitution; Fragmentation; 10 h; Title compound not separated from byproducts;
参考文献
Coe, Paul L.; Owen, Ian R.; Till, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 10 p. 1529 - 1535
参考文献
Tetrahedron, , vol. 27, p. 1221 - 1226
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 437 - 442
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 466 - 472
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 8, p. 235 - 242
反应条件
n-butyllithium 1) ether, -70 deg C, 30 min, 2) ether, 30 min; Yield given. Multistep reaction;
参考文献
Sauter, Fritz; Stanetty, Peter; Ramer, Wolfgang; Sittenthaler, Wilhelm
Monatshefte fuer Chemie, 1991 , vol. 122, # 10 p. 879 - 885