3,3-二乙氧基-2-甲基丙酸乙酯合成路线 （共 8 条）
反应条件
chloro-trimethyl-silane; zinc in diethyl ether Reformatsky reaction; 1 h; Heating;
参考文献
Bouhadir, Kamal H.; Zhou, Jing-Lan; Shevlin, Philip B.
Synthetic Communications, 2005 , vol. 35, # 7 p. 1003 - 1010
反应条件
sodium ethanolate T=0°C; Yield given;
参考文献
Tietze, Lutz-F.; Meier, Heinrich; Voss, Edgar
Synthesis, 1988 , # 4 p. 274 - 277
反应条件
1: 0 deg C to room temp., 3 h; room temp., 10 h 2: C2H5ONa / 0 °C View Scheme
参考文献
Tietze, Lutz-F.; Meier, Heinrich; Voss, Edgar
Synthesis, 1988 , # 4 p. 274 - 277
参考文献
Tschitschibabin
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1906 , vol. 38, p. 338
Chem. Zentralbl., 1906 , vol. 77, # II p. 758
参考文献
Tschitschibabin
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1906 , vol. 38, p. 338
Chem. Zentralbl., 1906 , vol. 77, # II p. 758
参考文献
Coffen; Schaer; Bizzarro; Cheung
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 296 - 300
反应条件
phosphoric acid
T=100°C; 1 h;
参考文献
Hodgkiss; Jones; Long; Middleton; Parrick; Stratford; Wardman; Wilson
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2268 - 2274
反应条件
lithium aluminium tetrahydride; diethyl ether
anschliessende Hydrolyse sowie Isolierung als 2,4-Dinitro-phenylhydrazon (F:158-161grad);
参考文献
Swoboda
Monatshefte fuer Chemie, 1951 , vol. 82, p. 388
