(R)-(+)-N-乙酰基-甲基苄胺合成路线 （共 87 条）
反应条件
Novozymereg;435; hydrogen in toluene T=70°C; 35 h; Enzymatic reaction; chemoselective reaction;
参考文献
Journal of Catalysis, , vol. 291, p. 87 - 94
反应条件
Novozymereg;435; hydrogen in toluene T=70°C; 25 h; Enzymatic reaction; chemoselective reaction;
参考文献
Journal of Catalysis, , vol. 291, p. 87 - 94
反应条件
Novozymereg;435; hydrogen in toluene T=70°C; 35 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Catalysis, , vol. 291, p. 87 - 94
反应条件
triethylamine in tetrahydrofuran T=20°C; 0.25 h;
参考文献
Tetrahedron, , vol. 68, # 21 p. 4013 - 4017
反应条件
Novozym 435 in toluene T=23°C; 6 h; Molecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 23, # 3-4 p. 230 - 236
反应条件
Candida antarctica lipase in di-isopropyl ether T=30°C; 120 h;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 44, # 6 p. 1312 - 1316
反应条件
1: H2 / Pd(OCOCF3)2; (S,S,R,R)-TangPhos / CH2Cl2 / 24 h / 40 °C / 57000 Torr 2: naphthalene; Na / 1,2-dimethoxy-ethane / 1 h / 20 °C 3: CH2Cl2 View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 23 p. 3832 - 3835
反应条件
1: m-CPBA / CH2Cl2 / 20 °C 2: H2 / Pd(OCOCF3)2; (S,S,R,R)-TangPhos / CH2Cl2 / 24 h / 40 °C / 57000 Torr 3: naphthalene; Na / 1,2-dimethoxy-ethane / 1 h / 20 °C 4: CH2Cl2 View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 23 p. 3832 - 3835
反应条件
Pseudomonas cepacia lipase PSL-C in various solvent(s) T=30°C; 32 h; Enzymatic reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 8-9 p. 1481 - 1488
反应条件
1: (E)-acetophenone O-acetyl oxime With Rh(cod)2SbF6; CyPF-tBu; hydrogen in 1,4-dioxane T=40°C; P=38002.6 Torr; 24 h; Autoclave; 2: acetic anhydride in 1,4-dioxane 0.5 h; Autoclave; SolventReagent/catalyst; Overall yield = 69 percentSpectr.; enantioselective reaction;
参考文献
Organic Letters, , vol. 15, # 3 p. 484 - 487
