(R)-(+)-N-乙酰基-甲基苄胺合成路线 (共 87 条)
反应条件
(Rp,S)-[2.2]paracyclophane-based N,O-ligand in hexane T=0 - 20°C; 16 h; Title compound not separated from byproducts.;
参考文献
Journal of the American Chemical Society, , vol. 124, # 21 p. 5940 - 5941
反应条件
N-Benzyldiacetamide; potassium hydride in diethylene glycol dimethyl ether T=120°C; 18 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 5 p. 761 - 763
反应条件
N-Benzyldiacetamide; potassium hydride in diethylene glycol dimethyl ether T=120°C; 18 h;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 5 p. 761 - 763
反应条件
hydrogen; Candida antarctica lipase B; Lindlar's catalyst in toluene T=70°C; P=75.0075 Torr; 24 h;
参考文献
Chemistry - A European Journal, , vol. 13, # 7 p. 2034 - 2043
反应条件
immobilized lipase B from Candida antarctica (CAL-B, Novozyme 435) in toluene T=110°C; 1 h; Inert atmosphereResolution of racemate;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
反应条件
immobilized lipase B from Candida antarctica (CAL-B, Novozyme 435) in toluene T=110°C; 1 h; Inert atmosphereResolution of racemate;
参考文献
Geukens, Inge; Plessers, Eva; Seo, Jin Won; De Vos, Dirk E.
European Journal of Inorganic Chemistry, 2013 , # 14 p. 2623 - 2628
反应条件
1: With n-butyllithium in tetrahydrofuran T=0°C; 2 h; 2: With sodium chloride Further stages.;
参考文献
Tetrahedron Asymmetry, , vol. 19, # 10 p. 1175 - 1181
反应条件
1: With n-butyllithium in tetrahydrofuran T=0°C; 2 h; 2: With sodium chloride Further stages.;
参考文献
Tetrahedron Asymmetry, , vol. 19, # 10 p. 1175 - 1181
反应条件
1: naphthalene; Na / 1,2-dimethoxy-ethane / 1 h / 20 °C 2: CH2Cl2 View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 23 p. 3832 - 3835
反应条件
n-butyllithium in tetrahydrofuran T=0°C;
参考文献
Tetrahedron Letters, , vol. 50, # 30 p. 4331 - 4334