N-甲苯磺酰基氮杂环丙烷合成路线 （共 27 条）
反应条件
nonafluoro-n-butanesulfonyl fluoride; triethylamine in dichloromethane T=20°C; 1 h;
参考文献
Yan, Zhaohua; Guan, Chengbo; Yu, Zhangxin; Tian, Weisheng
Tetrahedron Letters, 2013 , vol. 54, # 43 p. 5788 - 5790
反应条件
potassium hydroxide in water; toluene 2 h;
参考文献
Dietrich, Bernard; Hosseini, Mir Wais; Lehn, Jean-Marie; Sessions, Richard B.
Helvetica Chimica Acta, 1985 , vol. 68, p. 289 - 299
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane T=-20°C;
参考文献
Unthank, Matthew G.; Hussain, Nigel; Aggarwal, Varinder K.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 42 p. 7066 - 7069
反应条件
sodium hydroxide in water 1.5 h; Salt/ice bath;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA
Patent: WO2008/63721 A2, 2008 ;
Location in patent: Page/Page column 77 ;
反应条件
potassium hydroxide in tetrahydrofuran T=25°C; 0.0833333 h;
参考文献
Bates, Gordon S.; Ramaswamy, S.
Canadian Journal of Chemistry, 1980 , vol. 58, p. 716 - 722
反应条件
1: toluene-4-sulfonamide With sodium hydride in tetrahydrofuran T=20°C; 0.5 h; 2: diphenylvinyl sulfonium triflate in tetrahydrofuran T=20°C; 1 h;
参考文献
Yamanaka, Hiroyuki; Yamane, Yoshinobu; Mukaiyama, Teruaki
Heterocycles, 2004 , vol. 63, # 12 p. 2813 - 2826
反应条件
potassium hydroxide in dichloromethane; water T=20°C; 0.5 h;
参考文献
Bieber, Lothar W.; De Araujo, Maria C. F.
Molecules, 2002 , vol. 7, # 12 p. 902 - 906
反应条件
1: toluene-4-sulfonamide With sodium hydride in N,N-dimethyl-formamide T=20°C; 0.5 h; 2: (2-bromoethyl)(diphenyl)sulfonium trifluoromethanesulfonate With potassium iodide in N,N-dimethyl-formamide
参考文献
Heterocycles, , vol. 63, # 12 p. 2813 - 2826
反应条件
sodium hydroxide T=60°C; 15 h;
参考文献
Wamhoff, Heinrich; Thiemig, Heinz-Albrecht
Chemische Berichte, 1985 , vol. 118, # 11 p. 4473 - 4485
反应条件
{[2.1.1]-(2,6)-pyridinophane}CuCl2; Na[B(3,5-(CF3)2C6H3)4] in dichloromethane T=20°C; 0.0833333 h;
参考文献
Vedernikov, Andrei N.; Caulton, Kenneth G.
Organic Letters, 2003 , vol. 5, # 15 p. 2591 - 2594
