1,2-双(4-溴苯氧基)乙烷合成路线 （共 6 条）
反应条件
1: 4-bromo-phenol With sodium hydroxide in water
T=60 - 70°C; 0.5 h;
2: ethylene dibromide in water
T=100°C; 6 h;
参考文献
Zamadar, Matibur; Ghosh, Goutam; Mahendran, Adaickapillai; Minnis, Mihaela; Kruft, Bonnie I.; Ghogare, Ashwini; Aebisher, David; Greer, Alexander
Journal of the American Chemical Society, 2011 , vol. 133, # 20 p. 7882 - 7891
反应条件
bromine in acetic acid
1 h; Ambient temperature;
参考文献
Wilcox, Craig S.; Cowart, Marlon D.
Carbohydrate Research, 1987 , vol. 171, p. 141 - 160
反应条件
1: 1.2-dichloro-ethane; water
2: glacial acetic acid; bromine
View Scheme
参考文献
Cope
Journal of the American Chemical Society, 1935 , vol. 57, p. 572
参考文献
Cope
Journal of the American Chemical Society, 1935 , vol. 57, p. 572
反应条件
1: 4-bromo-phenol With sodium hydroxide in N,N-dimethyl-formamide
T=20°C; 0.5 h; Inert atmosphere;
2: 1,2-di(p-toluene-sulfonyloxy)ethane in N,N-dimethyl-formamide
T=80°C; Inert atmosphere;
参考文献
Yang, Hongyu; Xu, Minghua
Chinese Journal of Chemistry, 2013 , vol. 31, # 1 p. 119 - 122
参考文献
Cope
Journal of the American Chemical Society, 1935 , vol. 57, p. 572
