3-羟基-N-(4-甲基苯基)-2-萘甲酰胺合成路线 （共 8 条）
反应条件
phosphorus trichoride in chlorobenzene T=100 - 130°C; 0.75 h; Microwave irradiation;
参考文献
Kos, Jiri; Zadrazilova, Iveta; Pesko, Matus; Keltosova, Stanislava; Tengler, Jan; Gonec, Tomas; Bobal, Pavel; Kauerova, Tereza; Oravec, Michal; Kollar, Peter; Cizek, Alois; Kralova, Katarina; Jampilek, Josef
Molecules, 2013 , vol. 18, # 7 p. 7977 - 7997
反应条件
anhydrous phosphorus trichloride; sodium carbonate; urea in water; ethyl acetate; toluene
反应条件
acetic acid in 1,4-dioxane 2 h; Irradiation;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 7 p. 1363 - 1367
Zhurnal Organicheskoi Khimii, , vol. 19, # 7 p. 1514 - 1518
反应条件
acetic acid in 1,4-dioxane Irradiation;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 19, # 7 p. 1363 - 1367
Zhurnal Organicheskoi Khimii, , vol. 19, # 7 p. 1514 - 1518
参考文献
DE506837 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 696
参考文献
DE289027 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 12, p. 184
反应条件
1: 80 percent / tosyl azide, triethylamine / acetonitrile / 2 h / 25 °C
2: 84 percent / conc. aq. HCl / tetrahydrofuran / 0.83 h / Irradiation
View Scheme
参考文献
Erlikh, R. D.; Zaitseva, L. G.; Sarkisyan, A. Ts.; Partalla, N. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 7 p. 1363 - 1367
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1514 - 1518
反应条件
1: 80 percent / tosyl azide, triethylamine / acetonitrile / 2 h / 25 °C
2: 84 percent / conc. aq. HCl / tetrahydrofuran / 0.83 h / Irradiation
3: 62 percent / 190 °C
View Scheme
参考文献
Erlikh, R. D.; Zaitseva, L. G.; Sarkisyan, A. Ts.; Partalla, N. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 7 p. 1363 - 1367
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1514 - 1518
