1,3-二甲基-2-苯基-2H-苯并咪唑合成路线 （共 12 条）
反应条件
2,2'-azo-bisisobutyronitrile; 1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole in tetrahydrofuran T=61°C; 10 h; also in benzene; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 57, # 2 p. 662 - 666
反应条件
2,2'-azo-bisisobutyronitrile; 1,3-dimethyl-2-phenyl-2,3-dihydro-1H-benzo[d]imidazole in tetrahydrofuran T=61°C; 10 h; also in benzene; MechanismProduct distribution;
参考文献
Journal of Organic Chemistry, , vol. 57, # 2 p. 662 - 666
反应条件
sodium tetrahydroborate in methanol
T=20°C; 1 h;
参考文献
Hasegawa; Chiba; Nakajima; Suzuki; Yoneoka; Iwaya
Synthesis, 2001 , # 8 p. 1248 - 1252
反应条件
in tetrahydrofuran
11 h; Heating;
参考文献
Shi, Zhen; Gu, Huan
Synthetic Communications, 1996 , vol. 26, # 22 p. 4175 - 4179
反应条件
1: With sodium hydroxide in methanol
T=110°C;
2: With sodium tetrahydroborate in methanol
1 h; Further stages.;
参考文献
Lee, In-Sook Han; Kil, Hyun Joo; Ji, Young Ran
Journal of Physical Organic Chemistry, 2007 , vol. 20, # 7 p. 484 - 490
反应条件
acetic acid in methanol
0.5 h; Ambient temperature;
参考文献
Reddy, A. Pandu Ranga; Veeranagaiah, V.; Ratnam, C. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 367 - 371
反应条件
1: 4 N aq. sodium hydroxide / 0.33 h / Heating
2: conc. sulphuric acid / 4 h / Heating
3: 65 percent / glacial acetic acid / methanol / 0.5 h / Ambient temperature; other aromatic aldehydes
View Scheme
参考文献
Reddy, A. Pandu Ranga; Veeranagaiah, V.; Ratnam, C. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 367 - 371
参考文献
Krollpfeiffer; Graulich; Rosenberg
Justus Liebigs Annalen der Chemie, 1939 , vol. 542, p. 1,7
参考文献
Fischer,O.; Rigaud
Chemische Berichte, 1901 , vol. 34, p. 4203
Chemische Berichte, 1902 , vol. 35, p. 1258
参考文献
Smith et al.
Journal of the American Chemical Society, 1949 , vol. 71, p. 1082
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Krollpfeiffer; Graulich; Rosenberg
Justus Liebigs Annalen der Chemie, 1939 , vol. 542, p. 1,7
