2,4-二硝基-N-(壬烷-5-亚基氨基)苯胺合成路线 （共 18 条）
反应条件
1: m-chloroperbenzoic acid / CH2Cl2
2: 50 percent / butyl-lithium / hexane; tetrahydrofuran / 1 h / 0 °C
3: 86 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating
4: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C
View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C
View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: 86 percent / di-isobutylaluminum hydride / toluene / 48 h / Heating
2: 85percent m-chloroperbenzoic acid / CH2Cl2 / 1.5 h / -23 °C
View Scheme
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
反应条件
1: BTMACB; acetic acid; potassium bromide / water / 10 h / 298 °C / |Darkness
2: hydrogenchloride / water / |Cooling
View Scheme
参考文献
Sharma, Pradeep K.
Asian Journal of Chemistry, 2014 , vol. 26, # 9 p. 2702 - 2706
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 183 - 194
反应条件
1: ethanol; barium oxide; hydrazine hydrate
2: ethanol
View Scheme
参考文献
Braddock; Willard
Journal of Organic Chemistry, 1953 , vol. 18, p. 313
参考文献
Braddock; Willard
Journal of Organic Chemistry, 1953 , vol. 18, p. 313
反应条件
Yield given. Multistep reaction;
参考文献
Ager, David J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 195 - 204
