萘并(1,8-cd)-1,2-二硒杂环戊烯合成路线 （共 23 条）
反应条件
1: With n-butyllithium in tetrahydrofuran
T=-78 - 20°C; 1.5 h; Inert atmosphere;
2: With selenium in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
Press, David J.; Back, Thomas G.; Sutherland, Todd C.
Tetrahedron Letters, 2012 , vol. 53, # 13 p. 1603 - 1605
反应条件
Na2Se2 in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=100°C;
参考文献
Yui, Koji; Aso, Yoshio; Otsubo, Tetsuo; Ogura, Fumio
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 953 - 960
反应条件
dibenzoyl peroxide in tetrachloromethane
T=-20°C; 12 h;
参考文献
Fujihara, Hisashi; Saito, Rei; Yabe, Masayoshi; Furukawa, Naomichi
Chemistry Letters, 1992 , # 8 p. 1437 - 1440
反应条件
1: With n-butyllithium; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=70°C; 2 h; Inert atmosphere;
2: With selenium in tetrahydrofuran
T=-70 - 20°C; Inert atmosphere;
参考文献
Fuller, Amy L.; Knight, Fergus R.; Slawin, Alexandra M. Z.; Woollins, J. Derek
European Journal of Inorganic Chemistry, 2010 , # 25 p. 4034 - 4043
反应条件
in chloroform
T=15°C; Irradiation;
参考文献
Fujihara; Yabe; Chiu; Furukawa
Tetrahedron Letters, 1991 , vol. 32, # 34 p. 4345 - 4348
反应条件
trifluoroacetic anhydride in benzene
Ambient temperature;
参考文献
Fujihara, Hisashi; Saito, Rei; Yabe, Masayoshi; Furukawa, Naomichi
Chemistry Letters, 1992 , # 8 p. 1437 - 1440
反应条件
in chloroform; benzene
T=20°C; Elimination; addition; 3 h; Irradiation;
参考文献
Kobayashi, Kenji; Shinhara, Satoshi; Moriyama, Masaya; Fujii, Takayoshi; Horn, Ernst; Yabe, Akira; Furukawa, Naomichi
Tetrahedron Letters, 1999 , vol. 40, # 28 p. 5211 - 5214
反应条件
in chloroform; benzene
T=20°C; Elimination; addition; 3 h; Irradiation;
参考文献
Kobayashi, Kenji; Shinhara, Satoshi; Moriyama, Masaya; Fujii, Takayoshi; Horn, Ernst; Yabe, Akira; Furukawa, Naomichi
Tetrahedron Letters, 1999 , vol. 40, # 28 p. 5211 - 5214
反应条件
in chloroform; benzene
T=20°C; Elimination; addition; 3 h; Irradiation;
参考文献
Kobayashi, Kenji; Shinhara, Satoshi; Moriyama, Masaya; Fujii, Takayoshi; Horn, Ernst; Yabe, Akira; Furukawa, Naomichi
Tetrahedron Letters, 1999 , vol. 40, # 28 p. 5211 - 5214
反应条件
in chloroform
48 h; Ambient temperature;
参考文献
Fujihara, Hisashi; Yabe, Masayoshi; Furukawa, Naomichi
Journal of Organic Chemistry, 1993 , vol. 58, # 20 p. 5291 - 5292
