N-(1,2,2,2-四氯乙基)甲酰胺合成路线 （共 5 条）
反应条件
hydrogenchloride; sodium hydroxide; sodium chloride; NaOAc·3H2O in water; acetone
参考文献
Celamerck GmbH and Co. KG
Patent: US3975527 A1, 1976 ;
反应条件
thionyl chloride in toluene
3 h; Heating;
参考文献
Vrabel, Viktor; Pavelcik, Frantisek; Kelloe, Eleonora; Miertus, Stanislav; Konecny, Vaclav; Lokaj, Jan
Collection of Czechoslovak Chemical Communications, 1985 , vol. 50, # 8 p. 1619 - 1628
参考文献
Chamberlain; Summers
Australian Journal of Chemistry, 1974 , vol. 27, # 7 p. 1579 - 1583
反应条件
sodium hydroxide in water; toluene
T=20 - 25°C; 0.25 h;
参考文献
Vrabel, Viktor; Pavelcik, Frantisek; Kelloe, Eleonora; Miertus, Stanislav; Konecny, Vaclav; Lokaj, Jan
Collection of Czechoslovak Chemical Communications, 1985 , vol. 50, # 8 p. 1619 - 1628
反应条件
in dichloromethane
T=35°C; 2 h;
参考文献
Scheidecker, S.; Koeckritz, A.; Schnell, M.
Journal fuer Praktische Chemie (Leipzig), 1990 , vol. 332, # 6 p. 968 - 976
