4-羟基-2,3,6-三甲基乙酸苯酯合成路线 （共 22 条）
反应条件
peracetic acid
T=70°C; 4 h; Product distributionKineticsThermodynamic data;
参考文献
Kharchuk, V. G.; Kolenko, I. P.; Petrov, L. A.; Gus'kova, L. M.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 11 p. 2071 - 2078
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 11 p. 2306 - 2315
反应条件
1: 4-hydroxy-2,3,6-trimethylphenyl acetate With sodium hydride in tetrahydrofuran
T=2 - 3°C; 0.5 h;
2: (E/Z)-crotyl bromide in tetrahydrofuran
T=21 - 23°C; 18 h; Title compound not separated from byproducts;
参考文献
Malaise, Gregory; Bonrath, Werner; Breuninger, Manfred; Netscher, Thomas
Helvetica Chimica Acta, 2006 , vol. 89, # 4 p. 797 - 812
