N,N,N',N'-四甲基联苯胺合成路线 (共 97 条)
反应条件
oxygen; triethylamine; [Cu3(1,3,5-benzenetricarboxylate)2] in dichloromethane T=20°C; 5 h; Product distribution / selectivity;
参考文献
WO2011/14503 A1, ;
Page/Page column 23-28 ;
反应条件
1: With Cu(II) perchlorate in acetonitrile T=24 - 26°C; 10 h; 2: With potassium carbonate T=24 - 26°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 26 p. 9849 - 9852
反应条件
1: With antimony(V) pentachloride in dichloromethane T=20°C; 24 h; Inert atmosphere; 2: in dichloromethane T=20°C; 1 h; Inert atmosphereRefluxAlkaline conditions; Concentration;
参考文献
Arkivoc, , vol. 2013, # 3 p. 36 - 48
反应条件
N-fluoro-N-(phenylsulfonyl)benzene-sulfonamide in chloroform T=25°C; 10 h; TimeTemperatureReagent/catalyst;
参考文献
Journal of Fluorine Chemistry, , vol. 154, p. 67 - 72
反应条件
titanium tetrachloride in dichloromethane T=0 - 25°C; 5.5 h;
参考文献
Tetrahedron Letters, , vol. 44, # 50 p. 8939 - 8941
反应条件
titanium tetrachloride in dichloromethane T=0 - 25°C; 5.5 h;
参考文献
Tetrahedron Letters, , vol. 44, # 50 p. 8939 - 8941
反应条件
titanium tetrachloride in dichloromethane T=0 - 25°C; 5.5 h;
参考文献
Tetrahedron Letters, , vol. 44, # 50 p. 8939 - 8941
反应条件
trifluoroacetic acid; cobalt(II) dibromide; zinc dibromide in acetonitrile the mixt. in CH3CN was stirred at room temp., then arylbromide was added, stirred at room temp.; GC analysis;
参考文献
Journal of the American Chemical Society, , vol. 125, # 13 p. 3867 - 3870
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; palladium diacetate; N(Et)4ClO4; potassium carbonate in water; acetonitrile T=20°C; Inert atmosphereElectrochemical reaction;
参考文献
Tetrahedron, , vol. 65, # 40 p. 8384 - 8388
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI in tetrahydrofuran; benzene T=63°C; 3 h; Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 20 p. 4844 - 4848