N-(4-氟苯基)苯甲酰胺合成路线 （共 29 条）
反应条件
oxygen; potassium hydroxide in water
T=50°C; 12 h; Green chemistry;
参考文献
Guo, Xuefeng; Tang, Lin; Yang, Yu; Zha, Zhenggen; Wang, Zhiyong
Green Chemistry, 2014 , vol. 16, # 5 p. 2443 - 2447
反应条件
1: acetone / 2 h / 20 °C
2: 13 percent / NaOH / H2O / 20 h / 90 °C
View Scheme
参考文献
Saxena, Anil K.; Pandey, Suresh K.; Seth; Singh; Dikshit; Carpy
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 8 p. 2025 - 2034
反应条件
2,6-dimethylpyridine in water
T=80°C; 0.25 h; Microwave irradiation;
参考文献
Sharma, Pallavi; Moorhouse, Adam D.; Moses, John E.
Synlett, 2011 , # 16 art. no. D23011ST, p. 2384 - 2386
反应条件
1.1: 87 percent / thionyl chloride / 0 - 20 °C
2.1: n-butyl lithium / hexane / 1 h / 20 °C
2.2: 71 percent / hexane / 12 h / 20 °C
View Scheme
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
1: acetone / 2 h / 20 °C
2: 13 percent / NaOH / H2O / 20 h / 90 °C
View Scheme
参考文献
Saxena, Anil K.; Pandey, Suresh K.; Seth; Singh; Dikshit; Carpy
Bioorganic and Medicinal Chemistry, 2001 , vol. 9, # 8 p. 2025 - 2034
反应条件
diethyl ether; phosphorus pentachloride
und beim Behandeln mit Wasser;
参考文献
Bergmann; Hoffmann; Meyer
Journal fuer Praktische Chemie (Leipzig), 1932 , vol. <2> 135, p. 245,252
反应条件
1: AlCl3
3: phosphorus (V)-chloride; diethyl ether / und beim Behandeln mit Wasser
View Scheme
参考文献
Bergmann; Hoffmann; Meyer
Journal fuer Praktische Chemie (Leipzig), 1932 , vol. <2> 135, p. 245,252
反应条件
Eintragen des Reaktionsgemisches in Eis;
参考文献
Bergmann; Hoffmann; Meyer
Journal fuer Praktische Chemie (Leipzig), 1932 , vol. <2> 135, p. 245,252
反应条件
1.1: PCl5 / Heating
2.1: Na / ethanol / 1 h / 50 °C
2.2: toluene / 110 °C
3.1: 4.29 g / 170 °C
View Scheme
参考文献
Lai, Ya-Yun; Huang, Li-Jiau; Lee, Kuo-Hsiung; Xiao, Zhiyan; Bastow, Kenneth F.; Yamori, Takao; Kuo, Sheng-Chu
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 265 - 275
