双(三甲基硅基)亚磷酸盐合成路线 （共 20 条）
反应条件
in dichloromethane
T=20°C;
参考文献
Lewkowski, Jaroslaw; Karpowicz, Rafal
Heteroatom Chemistry, 2010 , vol. 21, # 5 p. 326 - 331
反应条件
in dichloromethane
T=20°C; 1.16667 h;
参考文献
Lewkowski, JarosLaw; Karpowicz, Rafa; Skowronski, Romuald
Phosphorus, Sulfur and Silicon and the Related Elements, 2009 , vol. 184, # 4 p. 815 - 819
反应条件
orthophosphorus acid
参考文献
Lebedev,E.P. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1977 , vol. 47, # 4 p. 765 - 769,698 - 701
Full Text Show Details
Yang, Ting; Lin, Changxue; Fu, Hua; Jiang, Yuyang; Zhao, Yufen
Synthetic Communications, 2004 , vol. 34, # 6 p. 1017 - 1022
参考文献
Voronkov,M.G. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 1987 - 1991,2005 - 2008
反应条件
2,2'-azo-bisisobutyronitrile; water
7 h; Reflux;
参考文献
Voronkov; Pestunovich; Albanov; Kukhareva
Russian Journal of General Chemistry, 2009 , vol. 79, # 6 p. 1080 - 1082
反应条件
in benzene
Heating; Product distribution;
参考文献
Livantsov, M. V.; Prishchenko, A. A.; Lutsenko, I. F.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 10 p. 2226 - 2233,1976 - 1982
反应条件
in benzene
Heating; Product distribution;
参考文献
Livantsov, M. V.; Prishchenko, A. A.; Lutsenko, I. F.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 10 p. 2226 - 2233,1976 - 1982
反应条件
water
1.) 130-140 deg C, 8 h; 2.) MeOH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Issleib, Kurt; Balszuweit, Arno; Richter, Hans-Juergen; Tonk, Walter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 12 p. 434 - 436
反应条件
water
1.) 120-130 deg C, 6 h; 2.) EtOH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Issleib, Kurt; Balszuweit, Arno; Richter, Hans-Juergen; Tonk, Walter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 12 p. 434 - 436
反应条件
water
1.) 130-140 deg C, 8 h; 2.) MeOH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Issleib, Kurt; Balszuweit, Arno; Richter, Hans-Juergen; Tonk, Walter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1983 , vol. 23, # 12 p. 434 - 436
