sulfuryl dichloride in dichloromethane T=20°C; 1 h; Inert atmosphere;

1: methanol 2: SOCl2 View Scheme

1: water / 0.17 h / 0 °C / |Inert atmosphere 2: sodium / ethanol / 2.17 h / 20 °C / |Inert atmosphere 3: sulfuryl dichloride / N,N-dimethyl-formamide / 4 h / 20 °C / |Reflux; |Inert atmosphere View Scheme

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / -15 °C / |Inert atmosphere 1.2: 1 h / -15 - 0 °C / |Inert atmosphere 2.1: water / 0.17 h / 0 °C / |Inert atmosphere 3.1: sodium / ethanol / 2.17 h / 20 °C / |Inert atmosphere 4.1: sulfuryl dichloride / N,N-dimethyl-formamide / 4 h / 20 °C / |Reflux; |Inert atmosphere View Scheme

1: chloroform 2: methanol 3: SOCl2 View Scheme

暂无反应条件数据

暂无反应条件数据

暂无反应条件数据