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乙二醇
甲醛
63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
366803-54-5
合成路线
（共 7 条）
909281-87-4
→
反应条件
366803-54-5
反应条件
hydrogen; palladium hydroxide on carbon in methanol T=20°C; 16 h;
参考文献
ZINGOTX PTY LTD
Patent: WO2006/125276 A1, 2006 ;
Location in patent: Page/Page column 26; 29 ;
223801-43-2
→
反应条件
366803-54-5
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran / 2 h / -80 - 20 °C 1.2: tetrahydrofuran / 5 h / -80 °C 1.3: 85 percent / aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating 2.1: 92 percent / H2 / Pd/C / ethyl acetate / 4 h / 20 °C View Scheme
参考文献
Tran, Van H.; Kantharaj, Ravi; Roufogalis, Basil D.; Duke, Colin C.
European Journal of Organic Chemistry, 2006 , # 13 p. 2970 - 2976
112-31-2
正癸醛
→
反应条件
366803-54-5
反应条件
1.1: 94 percent / NaHSO3 / H2O; methanol / 16 h / 20 °C 2.1: lithium diisopropylamide / tetrahydrofuran / 2 h / -80 - 20 °C 2.2: tetrahydrofuran / 5 h / -80 °C 2.3: 85 percent / aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating 3.1: 92 percent / H2 / Pd/C / ethyl acetate / 4 h / 20 °C View Scheme
参考文献
Tran, Van H.; Kantharaj, Ravi; Roufogalis, Basil D.; Duke, Colin C.
European Journal of Organic Chemistry, 2006 , # 13 p. 2970 - 2976
2426-87-1
4-苄氧基-3-甲氧基苯甲醛
→
反应条件
366803-54-5
反应条件
1.1: potassium tert-butoxide / tetrahydrofuran / 0.5 h / 0 °C 1.2: 78 percent / tetrahydrofuran / 6 h / 20 °C 2.1: 60 percent / aq. HCl / tetrahydrofuran / 3 h / Heating 3.1: lithium diisopropylamide / tetrahydrofuran / 2 h / -80 - 20 °C 3.2: tetrahydrofuran / 5 h / -80 °C 3.3: 85 percent / aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating 4.1: 92 percent / H2 / Pd/C / ethyl acetate / 4 h / 20 °C View Scheme
参考文献
Tran, Van H.; Kantharaj, Ravi; Roufogalis, Basil D.; Duke, Colin C.
European Journal of Organic Chemistry, 2006 , # 13 p. 2970 - 2976
16209-52-2
→
反应条件
366803-54-5
反应条件
1.1: lithium diisopropylamide / tetrahydrofuran / 2 h / -80 - 20 °C 1.2: tetrahydrofuran / 5 h / -80 °C 1.3: 85 percent / aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating 2.1: 92 percent / H2 / Pd/C / ethyl acetate / 4 h / 20 °C View Scheme
参考文献
Tran, Van H.; Kantharaj, Ravi; Roufogalis, Basil D.; Duke, Colin C.
European Journal of Organic Chemistry, 2006 , # 13 p. 2970 - 2976
121-33-5
香草醛
→
反应条件
366803-54-5
反应条件
1.1: 92 percent / NaH / dimethylformamide / 2 h / 20 °C 2.1: potassium tert-butoxide / tetrahydrofuran / 0.5 h / 0 °C 2.2: 78 percent / tetrahydrofuran / 6 h / 20 °C 3.1: 60 percent / aq. HCl / tetrahydrofuran / 3 h / Heating 4.1: lithium diisopropylamide / tetrahydrofuran / 2 h / -80 - 20 °C 4.2: tetrahydrofuran / 5 h / -80 °C 4.3: 85 percent / aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating 5.1: 92 percent / H2 / Pd/C / ethyl acetate / 4 h / 20 °C View Scheme
参考文献
Tran, Van H.; Kantharaj, Ravi; Roufogalis, Basil D.; Duke, Colin C.
European Journal of Organic Chemistry, 2006 , # 13 p. 2970 - 2976
210173-72-1
→
反应条件
366803-54-5
反应条件
1.1: 60 percent / aq. HCl / tetrahydrofuran / 3 h / Heating 2.1: lithium diisopropylamide / tetrahydrofuran / 2 h / -80 - 20 °C 2.2: tetrahydrofuran / 5 h / -80 °C 2.3: 85 percent / aq. oxalic acid / tetrahydrofuran / 1.5 h / Heating 3.1: 92 percent / H2 / Pd/C / ethyl acetate / 4 h / 20 °C View Scheme
参考文献
Tran, Van H.; Kantharaj, Ravi; Roufogalis, Basil D.; Duke, Colin C.
European Journal of Organic Chemistry, 2006 , # 13 p. 2970 - 2976
