1,1,2,2-四甲基-二膦合成路线 （共 33 条）
反应条件
in toluene
stirring, 2 h, under N2; concn., cooling to -10°C; elem. anal.;
参考文献
Berg, David J.; Andersen, Richard A.; Zalkin, Allan
Organometallics, 1988 , vol. 7, p. 1858 - 1863
反应条件
difluorosilylene; silicon tetrafluoride
T=-196°C; Substitution;
参考文献
Chang, Chih-Wei; Liu, Chao-Shiuan; Lee, Chi-Young
Journal of the Chinese Chemical Society, 1999 , vol. 46, # 3 p. 445 - 452
反应条件
in tetrahydrofuran
Heating;
参考文献
Bangerter,B.W. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 3247 - 3251
反应条件
in tetrahydrofuran
Heating;
参考文献
Bangerter,B.W. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 3247 - 3251
反应条件
in tetrahydrofuran
Heating;
参考文献
Bangerter,B.W. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 3247 - 3251
反应条件
in benzene
T=75°C; 6 h;
参考文献
Fritz, Gerhard; Bauer, Heinz
Angewandte Chemie, 1983 , vol. 95, # 9 p. 740 - 741
反应条件
in hexane
under N2 in a glove box, addn. of Li salt to Ti(NEt2)3Cl soln., stirring, colour change to orange brown; not isolated, react. monitored via NMR spect.;
参考文献
Dick, David G.; Rousseau, Roger; Stephan, Douglas W.
Canadian Journal of Chemistry, 1991 , vol. 69, # 2 p. 357 - 362
反应条件
in hexane
under N2 in a glove box, addn. of Li salt to Ti(NMe2)3Cl soln., stirring, colour change to orange brown; not isolated, react. monitored via NMR spect.;
参考文献
Dick, David G.; Rousseau, Roger; Stephan, Douglas W.
Canadian Journal of Chemistry, 1991 , vol. 69, # 2 p. 357 - 362
参考文献
Burg
Journal of Inorganic and Nuclear Chemistry, 1959 , vol. 11, p. 258
反应条件
magnesium
T=326.9°C; Further byproducts given;
参考文献
Bock, H.; Bankmann, M.
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 167 - 191
