4-氨基-2,2,6,6-四甲基哌啶合成路线 （共 35 条）
反应条件
in acetonitrile T=25°C; Equilibrium constant;
参考文献
Goermar, Gerhard; Seiffarth, Klaus; Schulz, Manfred; Chachimbombo, Chitula Leopoldina
Journal fuer Praktische Chemie (Leipzig), 1991 , vol. 333, # 3 p. 475 - 479
反应条件
T=130 - 140°C; im Rohr;
参考文献
Harries
Justus Liebigs Annalen der Chemie, 1918 , vol. 417, p. 176
参考文献
Harries
Justus Liebigs Annalen der Chemie, 1918 , vol. 417, p. 176
参考文献
Harries
Justus Liebigs Annalen der Chemie, 1918 , vol. 417, p. 176
反应条件
1.1: 197 g / diethyl ether / 3.5 h / 5 - 10 °C 2.1: K2CO3 / H2O / 0.25 h / 25 °C 2.2: 150.8 g / H2O2; sodium tungstate; disodium EDTA / H2O / 73 h 3.1: 49 percent / KOH / H2O / 29 h / Heating 4.1: 67 percent / Et3N / benzene / 20 °C View Scheme
参考文献
Plessas; Goldstein
Carbohydrate research, 1981 , vol. 89, # 2 p. 211 - 220
反应条件
sodium hydroxide in water; isopropyl alcohol T=30 - 130°C; P=1125.11 - 2475.25 Torr; Alkaline aqueous solution;
参考文献
WO2004/16591 A1, ;
Page/Page column 6-7 ;
反应条件
sodium hydroxide; acetic anhydride in water; isopropyl alcohol; toluene
参考文献
Ciba-Geigy Corporation
Patent: US5286865 A1, 1994 ;
反应条件
in diethyl ether T=5 - 10°C; 3.5 h;
参考文献
Zakrzewski, Jerzy; Krawczyk, Maria
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 1 p. 514 - 516
反应条件
sodium nitrite in water
参考文献
Kashparova; Kagan; Kashparov; Zhukova
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 4 p. 667 - 668
反应条件
hydrogenchloride; sodium nitrite in water pH=3 - 5;
参考文献
Kashparova; Kagan; Kashparov; Zhukova
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 4 p. 667 - 668
