反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride
1.) ethyl acetate, reflux, 9h; 2.) column chromatography; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Gioanola, Milena; Leardini, Rino; Nanni, Daniele; Pareschi, Patrizia; Zanardi, Giuseppe
Tetrahedron, 1995 , vol. 51, # 7 p. 2039 - 2054
