3,5-二甲基吡啶N-氧化物合成路线 （共 13 条）
反应条件
peracetic acid T=85°C; 2 h;
参考文献
Klan, P.
Monatshefte fuer Chemie, 1993 , vol. 124, # 3 p. 327 - 330
反应条件
peracetic acid; sodium hydroxide in chloroform; water; acetic acid
参考文献
CL Pharma Aktiengesellschaft
Patent: US5066810 A1, 1991 ;
反应条件
1.1: sulfuric acid; nitric acid / 6 h / 20 - 90 °C 2.1: palladium 10 on activated carbon / ethanol / 1 h / 90 °C / Inert atmosphere 2.2: 3 h / 90 °C / Inert atmosphere 3.1: phosphorus trichoride / chloroform / 22 h / 80 °C / Inert atmosphere View Scheme
参考文献
Fortage, Jerome; Peltier, Cyril; Perruchot, Christian; Takemoto, Yohei; Teki, Yoshio; Bedioui, Fethi; Marvaud, Valerie; Dupeyre, Gregory; Pospisil, Lubomir; Adamo, Carlo; Hromadova, Magdalena; Ciofini, Ilaria; Laine, Philippe P.
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2691 - 2705
反应条件
1: CH2Cl2 / Heating 2: conc. HCl View Scheme
参考文献
GLAXO GROUP LIMITED; BIRAULT, Véronique; CAMPBELL, Amanda, Jennifer; HARRISON, Stephen; LE, Joelle; SHUKLA, Lena
Patent: WO2013/160419 A1, 2013 ;
反应条件
triphenylphosphine; N-fused tetraphenylporphyrin rhenium(VII) trioxide in dichloromethane T=23°C; 6 h;
参考文献
Toganoh, Motoki; Fujino, Keitaro; Ikeda, Shinya; Furuta, Hiroyuki
Tetrahedron Letters, 2008 , vol. 49, # 9 p. 1488 - 1491
反应条件
in acetonitrile T=81°C; 4 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 44, # 2 p. 487 - 489
反应条件
mercury(II) diacetate; bromine; acetic acid T=70°C; 10 h; effect of metal ions; Product distributionMechanism;
参考文献
Monatshefte fuer Chemie, , vol. 124, # 3 p. 327 - 330
反应条件
1: in tetrahydrofuran T=25°C; 2: With acetic anhydride T=120°C; 0.0666667 h; microwave irradiation; Further stages.;
参考文献
Andersson, Hans; Almqvist, Fredrik; Olsson, Roger
Organic Letters, 2007 , vol. 9, # 7 p. 1335 - 1337
反应条件
sulfuric acid; nitric acid T=20 - 90°C; 6 h;
参考文献
Fortage, Jerome; Peltier, Cyril; Perruchot, Christian; Takemoto, Yohei; Teki, Yoshio; Bedioui, Fethi; Marvaud, Valerie; Dupeyre, Gregory; Pospisil, Lubomir; Adamo, Carlo; Hromadova, Magdalena; Ciofini, Ilaria; Laine, Philippe P.
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2691 - 2705
反应条件
bromine; Neutral lead acetate; acetic acid
T=70°C; 10 h;
参考文献
Klan, P.
Monatshefte fuer Chemie, 1993 , vol. 124, # 3 p. 327 - 330
