双(三氟甲基)二硫化物合成路线 (共 250 条)
参考文献
Munavalli; Rossman; Rohrbaugh; Ferguson; Durst
Journal of Fluorine Chemistry, 1996 , vol. 76, # 1 p. 7 - 13
参考文献
Sprenger; Shreeve
Journal of Fluorine Chemistry, 1974 , vol. 4, p. 201,202,204
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Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.9, page 243 - 251
反应条件
byproducts: MnCl2, CO;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
参考文献
Middleton,W.J. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1375 - 1384
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Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.6, page 195 - 217
反应条件
chlorine at -74°C; detection of products by IR-spectroscopy;
参考文献
Emeleus, H. J.; Nabi, S. N.
Journal of the Chemical Society, 1960 , p. 1103 - 1108
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Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.10, page 27 - 31
反应条件
pyrolysis at 400°C, at 1-1.5 Torr pressure;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.9, page 2 - 27
反应条件
byproducts: HCl; Irradiation (UV/VIS);
参考文献
Harris, J. F.
Journal of Organic Chemistry, 1981 , vol. 46, # 2 p. 268 - 271
反应条件
sodium hydride 1.) Et2O, r.t., 15 h, 2.) Et2O, -78 deg; Yield given. Multistep reaction;
参考文献
Boese, Roland; Haas, Alois; Lieb, Max; Roeske, Ulrich
Chemische Berichte, 1994 , vol. 127, # 3 p. 449 - 456
反应条件
T=80 - 90°C; 6 h; Further byproducts given;
参考文献
Munavalli, S.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.; Buettner, L.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 15 - 20
反应条件
T=80 - 90°C; 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Munavalli; Rossman; Rohrbaugh; Ferguson; Durst
Journal of Fluorine Chemistry, 1996 , vol. 76, # 1 p. 7 - 13